934-26-9, 6-Chloro-3-hydrazinylpyridazin-4-amine is a pyridazine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
934-26-9, A MW vial was charged with 6-chloro-3-hydrazinylpyridazin-4-amine (Stepi 12.2) (475 mg, 2.98 mmol) and potassium acetate (467 mg, 4.76 mmol) in AcOH (5 mL). The MW vial was sealed and the resulting mixture was heated up and stirred at 170¡ãC for 4 hr. The reaction was cooled down to RT and concentrated under reduced pressure. The crude product was purified by silicagel column chromatography (NH3 1percent/CH2CI2/MeOH 1-3percent) to afford the title product (450 mg,2.451 mmol, 82percent yield). tR. 2.32 mm (HPLC 1); tR. 0.55 mm (LC-MS 2); ESl-MS: 184 [M+H] (LC-MS 2); ESl-MS: 182 [M-H] (LC-MS 2); R = 0.45 (CH2CI2/MeOH 9:1).
The synthetic route of 934-26-9 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; NOVARTIS AG; BLANK, Jutta; BORDAS, Vincent; COTESTA, Simona; GUAGNANO, Vito; RUEEGER, Heinrich; VAUPEL, Andrea; WO2014/191896; (2014); A1;,
Pyridazine – Wikipedia
Pyridazine | C4H4N2 – PubChem