Some tips on 20698-04-8

The synthetic route of 20698-04-8 has been constantly updated, and we look forward to future research findings.

20698-04-8, 3,6-Diiodopyridazine is a pyridazine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

3-Iodo-6-dimethylaminopyridazine can be prepared by stirring a solution of 3,6-diiodopyridazine (203.7 g) and dimethylamine (276 g) in methanol (1500 cc) at a temperature of about 20 C for 48 hours. After evaporation to dryness under reduced pressure, the residue obtained is stirred for 15 minutes with distilled water (1500 cc). The insoluble product is filtered off and washed with distilled water (2 * 200 cc). 6-Dimethylamino-3-iodopyridazine (113.7 g), melting at 135 C, is obtained.

The synthetic route of 20698-04-8 has been constantly updated, and we look forward to future research findings.

Reference£º
Patent; Rhone-Poulenc Industries; US4110450; (1978); A;,
Pyridazine – Wikipedia
Pyridazine | C4H4N2 – PubChem

 

Some tips on 20698-04-8

The synthetic route of 20698-04-8 has been constantly updated, and we look forward to future research findings.

20698-04-8, 3,6-Diiodopyridazine is a pyridazine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

3-Iodo-6-dimethylaminopyridazine can be prepared by stirring a solution of 3,6-diiodopyridazine (203.7 g) and dimethylamine (276 g) in methanol (1500 cc) at a temperature of about 20 C for 48 hours. After evaporation to dryness under reduced pressure, the residue obtained is stirred for 15 minutes with distilled water (1500 cc). The insoluble product is filtered off and washed with distilled water (2 * 200 cc). 6-Dimethylamino-3-iodopyridazine (113.7 g), melting at 135 C, is obtained.

The synthetic route of 20698-04-8 has been constantly updated, and we look forward to future research findings.

Reference£º
Patent; Rhone-Poulenc Industries; US4110450; (1978); A;,
Pyridazine – Wikipedia
Pyridazine | C4H4N2 – PubChem

 

Brief introduction of 20698-04-8

As the paragraph descriping shows that 20698-04-8 is playing an increasingly important role.

With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.20698-04-8,3,6-Diiodopyridazine,as a common compound, the synthetic route is as follows.

3-Iodo-6-dimethylaminopyridazine can be prepared by stirring, at a temperature of 20 C for 48 hours, a solution of 3,6-diiodopyridazine (203.7 g) and of dimethylamine (276 g) in methanol (1500 cc). After evaporation to dryness under reduced pressure, the residue obtained is stirred for 15 minutes with distilled water (1500 cc). The insoluble product is filtered off and washed with distilled water (2 * 200 cc) to give 3-iodo-6-dimethylaminopyridazine (113.7 g) melting at 135 C.

As the paragraph descriping shows that 20698-04-8 is playing an increasingly important role.

Reference£º
Patent; Rhone-Poulenc Industries; US4104386; (1978); A;,
Pyridazine – Wikipedia
Pyridazine | C4H4N2 – PubChem