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Homochiral (alphaMe)Leu/Ala and Leu/Ala model peptides were synthesized by solution methods and fully characterized.A solution conformational analysis of the tripeptides was carried out using FT-IR absorbtion and 1H NMR.The crystal-state structure of Z-D-(alphaMe)Leu-(D-Ala)2-OMe monohydrate was resolved by X-ray diffraction.The results obtained support the conclusion that the tendency of the non-coded (alphaMe)Leu residue to fold into beta-bends and helical structures is markedly higher than that of its unmethylated protein counterpart (Leu).
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Reference：
Pyridazine – Wikipedia,
Pyridazine | C4H4N2666 – PubChem