5469-70-5, 3-Aminopyridazine is a pyridazine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
5469-70-5, Example 24a 10774] 3-aminopyridazine (1 g, 10.5 mmol) is dissolved in toluene (7 mE) and N,N-dimethylformamide dimethyl acetal (1.8 mE, 13.67 mmol) is added. The mixture is heated at 65 C. and stirring is continued overnight. Additional N,N-dimethylformamide dimethyl acetal (1.8 mE, 13.67 mmol) is added and stirring is continued at it for 3 days. Additional N,N-dimethylformamide dimethyl acetal (3.6 mE, 27.34 mmol) is added and the reaction is heated at 85 C. for 5 h. Volatiles are removed under reduced pressure and the resulting residue is triturated with n-hexane to thmish the title compound (1.4 g, 91%)10775] UPEC-MS (Method 2): R=0.40 mm10776] MS (ESI pos): mlz=151 (M+H7
5469-70-5 3-Aminopyridazine 230373, apyridazine compound, is more and more widely used in various.
Reference£º
Patent; Boehringer Ingelheim International GmbH; GIOVANNINI, Riccardo; CUI, Yunhai; DOODS, Henri; FERRARA, Marco; JUST, Stefan; KUELZER, Raimund; LINGARD, Iain; MAZZAFERRO, Rocco; RUDOLF, Klaus; US2014/343065; (2014); A1;,
Pyridazine – Wikipedia
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