Discovery of 136725-55-8

When you point to this article, it is believed that you are also very interested in this compound(136725-55-8)Reference of (R)-(-)-3-Fluoropyrrolidine Hydrochloride and due to space limitations, I can only present the most important information.

In general, if the atoms that make up the ring contain heteroatoms, such rings become heterocycles, and organic compounds containing heterocycles are called heterocyclic compounds. An article called Scalable Process Design for a PDE10A Inhibitor Consisting of Pyrazolopyrimidine and Quinoxaline as Key Units, published in 2019-04-19, which mentions a compound: 136725-55-8, Name is (R)-(-)-3-Fluoropyrrolidine Hydrochloride, Molecular C4H9ClFN, Reference of (R)-(-)-3-Fluoropyrrolidine Hydrochloride.

In this study, research and development for the synthetic process of a PDE10A inhibitor are described; in particular, an efficient regioselective construction of the quinoxaline unit, a cost-effective pyrazolo[1,5-a]pyrimidine formation, and a cost-saving approach in a nucleophilic aromatic substitution (SNAr) reaction by introducing oxazolidinone as an electron-withdrawing group to a chloropyrazolo[1,5-a]pyrimidine core are key points. The newly developed process has been successfully scaled up to 40 kg. Furthermore, a one-pot tandem reaction from aminopyrazole to dichloropyrazolo[1,5-a]pyrimidine by activating malonic acid with POCl3 was discovered. The finding contributed to avoiding isolation of the hygroscopic pyrazolo[1,5-a]pyrimidin-5(4H)-one intermediate, which caused complicated filtration and drying processes observed in the first scale-up campaign.

When you point to this article, it is believed that you are also very interested in this compound(136725-55-8)Reference of (R)-(-)-3-Fluoropyrrolidine Hydrochloride and due to space limitations, I can only present the most important information.

Reference:
Pyridazine – Wikipedia,
Pyridazine | C4H4N2 – PubChem