50901-46-7, 1-(Pyridazin-4-yl)ethanone is a pyridazine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,50901-46-7
To 1-pyridazin-4-ylethanone (0.230 g) was added 1 , 1-dimethoxy-/V,/V-dimethyl-nnethanannine (0.275 ml_) and the mixture was heated at reflux for 1 hour, cooled to room temperature and allowed to stand overnight. The combined organic layers were concentrated and purified by silica gel chromatography eluting with 0 to 50% acetonitrile in dichloromethane to afford (E)-3-(dimethylamino)-1-pyridazin-4-yl- prop-2-en-1-one as an orange solid. (0933) NMR (400MHz, CDCIs) 9.57 – 9.53 (m, 1 H), 9.32 (dd, 1 H), 7.92 (d, 1 H), 7.84 (dd, 1 H), 5.66 (d, 1 H), 3.24 (s, 3H), 3.00 (s, 3H)
The synthetic route of 50901-46-7 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; SYNGENTA PARTICIPATIONS AG; SCUTT, James, Nicholas; WILLETTS, Nigel, James; SONAWANE, Ravindra; PHADTE, Mangala; KANDUKURI, Sandeep, Reddy; SASMAL, Swarnendu; ARMSTRONG, Sarah; MCGRANAGHAN, Andrea; (155 pag.)WO2019/185875; (2019); A1;,
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