35857-89-7, 6-Chloropyridazine-3-carbonitrile is a pyridazine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Of methyl (piperidin-4-yl) -carbamic acid tert-butyl ester (605.8mg, 2.83mmol) and 6-chloro-pyridazin-3-carbonitrile (796.5mg, 5.71mmol)In ethanol (15mL) was added triethylamine (1.14g, 11.30mmol). The reaction was stirred overnight at room temperature, and then concentrated under reduced pressure.The resulting residue was purified by silica gel column chromatography (EtOAc / PE (v / v) = 1/1) to give the title compound as a yellow solid (252.0mg, yield28.1%).
The synthetic route of 35857-89-7 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Guangdong East Sunshine Pharmaceutical Co., Ltd.; Xi, Ning; Li, Minxiong; Li, Xiaobo; Dai, Weilong; Hu, Haiyang; Zhang, Tao; Chen, Wuhong; (105 pag.)CN105461694; (2016); A;,
Pyridazine – Wikipedia
Pyridazine | C4H4N2 – PubChem