1632-76-4, 3-Methylpyridazine is a pyridazine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Synthesis of 6-methylpyridazine 1-oxideTo a solution of 3-methylpyridazine (4.60 g, 48.9 mmol) in acetic acid (30.0 mL) was added H202 (29.4 g,259 mmol, 29.4 mL, 30percent (w/w) in water). The mixture was heated at 120 ¡ãC for 6 h. The mixture wasallowed to cool to RT and poured in aqueous saturated NaHCO3 (500 mL) and extracted with DCM (5x 50 mL). The combined organic layer was dried over Na2SO4 and concentrated in vacuo to afford 6- methylpyridazine 1-oxide (2.22 g, 20.2 mmol, 41percent). LCMS: caic. for [M+H] = 111.05, found 111.2. 1H- NMR shows a 1:1 mixture of both possible N-oxides.
1632-76-4 3-Methylpyridazine 74208, apyridazine compound, is more and more widely used in various.
Reference£º
Patent; GRUeNENTHAL GMBH; NARDI, Antonio; RATCLIFFE, Paul; CRAAN, Tobias; HERTRAMPF, Thorsten; LESCH, Bernhard; KIME, Robert; STEINHAGEN, Henning; WO2015/161928; (2015); A1;,
Pyridazine – Wikipedia
Pyridazine | C4H4N2 – PubChem